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Thionyl Chloride → 5-(1-Chlorobutyl)-2-(2,6-diethyl-phenyl)-4-ethoxy-pyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 1-[6-(2,6-Diethyl-phenyl)-4-ethoxy-pyridin-3-yl]-butan-1-ol | HCID 59678316 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 5-(1-Chlorobutyl)-2-(2,6-diethyl-phenyl)-4-ethoxy-pyridine | HCID 66993937 | — |
反応手順
A mixture of 1-[6-(2,6-diethyl-phenyl)-4-ethoxy-pyridin-3-yl]-butan-1-ol (29 mg) and SOCl2 (0.2 mL) in CH2Cl2 (1 mL) is stirred at room temperature for one hour. The volatile materials are removed in vacuo to give 5-(1-chloro-butyl)-2-(2,6-diethyl-phenyl)-4-ethoxy-pyridine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07342115B2 |
| 出典データセット | uspto-grants-2008_03 |
| ORD ID | ord-9fffb10ea70e4cc49cf1de41802e8774 |
| 出典メモ | uspto-grants-2008_03 |