(Phenylmethyl)hydrazine → HCID 16045165, compound

HRID 1393247Notes

Reaction equation

HRID 1393247 reaction equation
[CH2:1]([NH:8][NH2:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Cl:10][C:11]1[CH:16]=[CH:15][C:14]([S:17]([N:20]2[CH:25]3[CH2:26][CH2:27][CH2:28][CH:21]2[C:22](=[CH:30]O)[C:23](=O)[CH2:24]3)(=[O:19])=[O:18])=[CH:13][CH:12]=1>>[CH2:1]([N:8]1[C:23]2[CH2:24][CH:25]3[N:20]([S:17]([C:14]4[CH:15]=[CH:16][C:11]([Cl:10])=[CH:12][CH:13]=4)(=[O:19])=[O:18])[CH:21]([CH2:28][CH2:27][CH2:26]3)[C:22]=2[CH:30]=[N:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 11157(Phenylmethyl)hydrazineHCID 668419749-(4-Chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one

Product 1

HCID 16045165HCID 16045165, compound

Procedure

Prepared as described in Example 5 using benzylhydrazine and 9-(4-chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one which was prepared as described in Example 34.

Workup

  1. customPrepared
  2. customwas prepared

Sources & evidence

ORD record
ord-f7408d4ed2724500b9bd802ecaa1bc7c
Source dataset
uspto-grants-2008_03
Patent number
US07345056B2

Reaction notes

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