Formamidine acetate → HCID 46884005, compound

HRID 1393261Notes

Reaction equation

HRID 1393261 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:11]2[CH:16]3[CH2:17][CH2:18][CH2:19][CH:12]2[C:13](=[CH:21]O)[C:14](=O)[CH2:15]3)(=[O:10])=[O:9])=[CH:4][CH:3]=1.C(O)(=O)C.[CH:27]([NH2:29])=[NH:28]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:11]2[CH:16]3[CH2:17][CH2:18][CH2:19][CH:12]2[C:13]2[CH:21]=[N:28][CH:27]=[N:29][C:14]=2[CH2:15]3)(=[O:10])=[O:9])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 160693Formamidine acetateHCID 668419749-(4-Chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one

Product 1

HCID 46884005HCID 46884005, compound

Procedure

Prepared as described in Example 5 using 9-(4-chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one which was prepared as described in Example 34 and formamidine acetate. See also: Hajos, Gyorgy; Snatzke, Guenther Liebigs Annalen der Chemie 1989, (1), 31-3.

Workup

  1. customPrepared
  2. customwas prepared

Sources & evidence

ORD record
ord-203a5ef5e2e4415fa24bf338f545be13
Source dataset
uspto-grants-2008_03
Patent number
US07345056B2

Reaction notes

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