HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Toluidine → HCID 53269524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Toluidine | HCID 7934 | — |
| Reactant | 4-Chloro-1,2-dinitrobenzene | HCID 33097 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53269524 | HCID 53269524 | — |
Reaction Steps
81 ml of m-toluidine is added to a solution of 50 g of 1-chloro-3,4-dinitrobenzene in 250 ml of ethanol, and the solution was allowed to stand for 72 hours. The reaction mixture was filtered, and the crystallizate was washed with cold ethanol and 2N aqueous hydrochloric acid. It was purified by chromatography on silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07345075B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-af0b12bf4bc14099973f49510c4d3045 |
| Source note | uspto-grants-2008_03 |