HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1393552Generated: October 30, 2026
3,4-Dimethoxyaniline → HCID 21937960, compound
https://huagongshe.com/reaction/1393552
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3,4-Dimethoxyaniline | HCID 22770 | — |
| Reactant | 3-Fluoro-4-nitrophenol | HCID 520948 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21937960 | HCID 21937960 | — |
Reaction Steps
3 g of 3-fluoro-4-nitrophenol and 8.8 g of 3,4-dimethoxyaniline were mixed and stirred for 2 hours at 150° C. After cooling, it was dissolved in dichloromethane and extracted twice with 1N aqueous hydrochloric acid. The aqueous phase was extracted twice with chloroform, and the combined chloroform extracts were dried on sodium sulfate and concentrated by evaporation in a vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07345075B2 |
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| Source dataset | uspto-grants-2008_03 |
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| ORD ID | ord-4b883021c9274626849b7f7b8f6affde |
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| Source note | uspto-grants-2008_03 |
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