1,3-Benzodioxol-5-amine → HCID 21938137, compound

HRID 1393553Notes

Reaction equation

HRID 1393553 reaction equation
F[C:2]1[CH:3]=[C:4]([OH:11])[CH:5]=[CH:6][C:7]=1[N+:8]([O-:10])=[O:9].[CH2:12]1[O:21][C:20]2[CH:19]=[CH:18][C:16]([NH2:17])=[CH:15][C:14]=2[O:13]1>>[CH2:12]1[O:21][C:20]2[CH:19]=[CH:18][C:16]([NH:17][C:2]3[CH:3]=[C:4]([OH:11])[CH:5]=[CH:6][C:7]=3[N+:8]([O-:10])=[O:9])=[CH:15][C:14]=2[O:13]1

Participants

3

Reactant 2

HCID 843101,3-Benzodioxol-5-amineHCID 5209483-Fluoro-4-nitrophenol

Product 1

HCID 21938137HCID 21938137, compound

Conditions

Temperature
120 °C

Procedure

0.86 g of 3-fluoro-4-nitrophenol and 2.25 g of 3,4-methylenedioxyaniline were mixed and stirred for 5 hours at 120° C. The raw mixture was chromatographed on silica gel.

Workup

  1. customThe raw mixture was chromatographed on silica gel

Sources & evidence

ORD record
ord-dc00ff1a0daf498f91153dbd3785e821
Source dataset
uspto-grants-2008_03
Patent number
US07345075B2

Reaction notes

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