HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1393587Generated: November 1, 2026
3,4-Dimethylaniline → 3-[(3,4-Dimethylphenyl)amino)-4,6-dinitrophenol
https://huagongshe.com/reaction/1393587
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3,4-Dimethylaniline | HCID 7248 | — |
| Reactant | 5-Fluoro-2,4-dinitrophenol | HCID 15083885 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-[(3,4-Dimethylphenyl)amino)-4,6-dinitrophenol | HCID 21938041 | — |
Reaction Steps
6.6 g of 3,4-dimethylaniline was added to a suspension that consists of 4 g of 4,6-dinitro-3-fluorophenol (J. Org. Chem. 1991, 5958) in 100 ml of ethanol, and it was stirred for 7 days at 40° C. After cooling, it was suctioned off, and the residue was recrystallized from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07345075B2 |
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| Source dataset | uspto-grants-2008_03 |
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| ORD ID | ord-b03ae106190c4cf68b5a7dd00b531ee0 |
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| Source note | uspto-grants-2008_03 |
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