HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → HCID 11600826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | 4-Thiazolidinecarboxamide | HCID 9964101 | — |
| Product | HCID 11600826 | HCID 11600826 | 59.1% |
Reaction Steps
In a similar procedure as employed in the Intermediate Example 1, the thiazolidine-4-carboxylic acid amide (102 mg) obtained above was reacted with chloroacetyl chloride (105 mg) and then subjected to dehydration reaction to give the title compound (87 mg, Y.:59%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07345180B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-ceacaa8bf6a54e019a9994089cd3012b |
| Source note | uspto-grants-2008_03 |