4-Nitrobenzenesulfonyl chloride → HCID 22456391, compound

HRID 1393866Notes

Reaction equation

HRID 1393866 reaction equation
Cl.[C:2]([O:6][C:7](=[O:10])[CH2:8][NH2:9])([CH3:5])([CH3:4])[CH3:3].[N+:11]([C:14]1[CH:19]=[CH:18][C:17]([S:20](Cl)(=[O:22])=[O:21])=[CH:16][CH:15]=1)([O-:13])=[O:12]>N1C=CC=CC=1>[N+:11]([C:14]1[CH:15]=[CH:16][C:17]([S:20]([NH:9][CH2:8][C:7]([O:6][C:2]([CH3:5])([CH3:4])[CH3:3])=[O:10])(=[O:22])=[O:21])=[CH:18][CH:19]=1)([O-:13])=[O:12]

Participants

4

Reactant 2

HCID 74044-Nitrobenzenesulfonyl chlorideHCID 2725036Glycine tert-butyl ester hydrochloride

Product 1

HCID 22456391HCID 22456391, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Glycine tert-butyl ester hydrochloride is reacted with 4-nitrobenzenesulfonyl chloride in pyridine, to give tert-butyl 2-{[(4-nitrophenyl)sulfonyl]amino}acetate.

Sources & evidence

ORD record
ord-b078ac831aed49e8a6afb4a5c58a528b
Source dataset
uspto-grants-2008_03
Patent number
US07348017B2

Reaction notes

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