Methanol → HCID 22938302, compound

HRID 1393874Notes

Reaction equation

HRID 1393874 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH2:14][C:15]([OH:17])=[O:16])[CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[C:9]=1[OH:10])([O-:3])=[O:2].S(=O)(=O)(O)O.[CH3:23]O>>[N+:1]([C:4]1[CH:5]=[C:6]([CH2:14][C:15]([O:17][CH3:23])=[O:16])[CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[C:9]=1[OH:10])([O-:3])=[O:2]

Participants

4

Reactant 3

HCID 887MethanolHCID 1118Sulfuric AcidHCID 985963,5-Dinitro-4-hydroxyphenacetic acid

Product 1

HCID 22938302HCID 22938302, compound

Procedure

3,5-Dinitro-4-hydroxyphenylacetic acid is refluxed in methanol in the presence of sulfuric acid, to give methyl 2-(3,5-dinitro-4-hydroxyphenyl)acetate.

Sources & evidence

ORD record
ord-2a6661b2ab5f4c4ba1eaac0bc5d64a2d
Source dataset
uspto-grants-2008_03
Patent number
US07348017B2

Reaction notes

Loading…