Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1394132Generated: November 3, 2026

HCID 69242804, compound → HCID 11675251, compound

https://huagongshe.com/reaction/1394132

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69242804HCID 69242804—
SolventHydrochloric AcidHCID 313—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 11675251HCID 11675251—

Reaction Steps

A solution of Example 18A (100 mg) in 4 M HCl in dioxane (2 mL) was stirred at room temperature for 16 hours, and concentrated under reduced pressure. The residue was taken up and concentrated under reduced pressure under the following solvents, methanol (10 mL), ether (10 mL) and dichloromethane (10 mL) to provide the titled compound as a pale yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07348346B2
Source datasetuspto-grants-2008_03
ORD IDord-accc1827dca6476cb51b4ecfd08d0c26
Source noteuspto-grants-2008_03