Ethylamine → HCID 59681801, compound

HRID 1394190Notes

Reaction equation

[NH2:1][C:2]1[C:3]([C:7]2[N:8]([CH2:24][CH3:25])[C:9]3[C:14]([C:15]4[CH:16]=[C:17]([CH:20]=[CH:21][CH:22]=4)[CH:18]=O)=[CH:13][N:12]=[CH:11][C:10]=3[N:23]=2)=[N:4][O:5][N:6]=1.[CH2:26]([NH2:28])[CH3:27]>>[CH2:24]([N:8]1[C:9]2[C:14]([C:15]3[CH:22]=[CH:21][CH:20]=[C:17]([CH2:18][NH:28][CH2:26][CH3:27])[CH:16]=3)=[CH:13][N:12]=[CH:11][C:10]=2[N:23]=[C:7]1[C:3]1[C:2]([NH2:1])=[N:6][O:5][N:4]=1)[CH3:25]

Participants

Reactant 2

HCID 6341Ethylamine

HCID 131726811HCID 131726811, compound

Product 1

HCID 59681801HCID 59681801, compound

Procedure

The product of Step 1 was converted into the title compound by reaction with ethylamine (1M in THF) according to the general method of Example 149. MS (ES+) m/e 364 [M+H]+.

Sources & evidence

ORD record: ord-9b62a59942824cae8e3de05da7f6f9d1
Source dataset: uspto-grants-2008_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07348339B2

Reaction notes

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