Methyl iodide → HCID 18538472, compound

Participants

Reaction Steps

A mixture of the compound obtained in Example 18 (310 mg, 0.60 mmol), methyl iodide (0.75 ml) and acetonitrile (10 ml) was stirred at room temperature for 14 hours. The reaction mixture was concentrated under reduced pressure. To the concentrate was added diethyl ether, and the resulting precipitates were collected by filtration. The precipitates were washed with diethyl ether, and dried under reduced pressure to give the titled compound (344 mg, 0.52 mmol, Yield 87%) as white amorphous substance.

Provenance & Evidence