HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Methoxyphenyl)boronic acid → HCID 16751732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Methoxyphenyl)boronic acid | HCID 2734370 | — |
| Reactant | HCID 16751727 | HCID 16751727 | — |
| Product | HCID 16751732 | HCID 16751732 | 54% |
Reaction Steps
The title compound was prepared in 54% yield according to the procedure described in Example 2, starting from 6-bromo-3,3-dimethyl-imidazo[1,2-a]pyridin-2-one and 3-methoxyphenyl boronic acid. 1H NMR (CDCl3) δ7.86 (dd, J=2.1 and 9.2 Hz, 1H), 7.73 (d, J=1.5 Hz, 1H), 7.43-7.39 (m, 1H), 7.28-7.25 (m, 1H), 7.05 (m, 1H), 6.97-6.94 (m, 2H), 3.88 (s, 3H), 1.63 (s, 6H); MS (m/e): 269 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07348432B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-782ae533bce84b30a9130617d3a65ff1 |
| Source note | uspto-grants-2008_03 |