HuagongsheHuagongshe Chemistry Print Report · For research reference only
Mesitylene → 5-Allyl-6-chloroindan-4-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Mesitylene | HCID 7947 | — |
| Reactant | 4-(Allyloxy)-6-chloroindane | HCID 68583970 | — |
| Product | 5-Allyl-6-chloroindan-4-ol | HCID 68585868 | 56% |
Reaction Steps
Treatment of 4-(allyloxy)-6-chloroindane (8.0 g, 0.038 mol) in refluxing mesitylene (270 mL) generally according to the procedure described for Intermediate 1 afforded 4.5 g (56%) of 5-allyl-6-chloroindan-4-ol as a colorless oil which solidified into a white solid upon standing. mp 37-39° C.; Anal. calcd. for C12H13ClO.0.1H2O: C, 68.48; H, 6.32. Found: C, 68.54; H, 6.29.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07728155B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-a22c5adcc1c84f2c827b68d9447ff539 |
| Source note | uspto-grants-2010_06 |