関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | p-Bromoacetophenone | HCID 7466 | — |
| 反応物 | N-(Carbobenzyloxy)-DL-proline | HCID 232388 | — |
| 試薬 | Cesium carbonate | HCID 10796 | — |
| 触媒 | 4,4'-Di-tert-butyl-2,2'-bipyridyl | HCID 4249187 | — |
| 触媒 | Dichloronickel;1,2-dimethoxyethane | HCID 15773433 | — |
| 触媒 | HCID 178441129 | HCID 178441129 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | HCID 126482334 | HCID 126482334 | 93% |
反応手順
Prior to irradiation, the reaction mixture was degassed by bubbling argon for 20 minutes
情報源と証拠
| DOI | 10.1126/science.1255525 |
|---|
| 出典データセット | Coupling of α-carboxyl sp3-carbons with aryl halides |
|---|
| ORD ID | ord-cf0d04017ede4c8aab8a15119c53e57b |
|---|
| 出典メモ | Coupling of α-carboxyl sp3-carbons with aryl halides |
|---|