HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 1-(Benzyloxy)-4,5-dimethoxy-2-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 1,2-Dimethoxy-4,5-dinitrobenzene | HCID 222989 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-(Benzyloxy)-4,5-dimethoxy-2-nitrobenzene | HCID 284047 | — |
Reaction Steps
When the formation of hydrogen had ceased (in about 30 min) 456 g (2 mole) of 1,2-dimethoxy-4,5-dinitrobenzene were added and the reaction mixture was refluxed for 2 h. To the solution, 4 l of methanol and 300 ml of water were added. Upon cooling in ice a precipitate was formed which was filtered off and dried. Yield: 369 g (64%); melting point: 141° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04201584 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-b88c9ce2ad294f04a53b8af048137194 |
| Source note | uspto-grants-1980_05 |