Sulfuric Acid → HCID 20341149, compound
Reaction equation
[CH2:1]([Cl:5])[C:2](=[CH2:4])[CH3:3].[CH2:6]=[CH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.S(=O)(=O)(O)O>>[CH2:6]=[CH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.[CH2:1]([Cl:5])[C:2](=[CH2:3])[CH3:4]Participants
4
Procedure
About 1 part by weight of fine granular hydrated silica, 2 parts by weight of methallyl chloride and 1 part by weight of styrene are mixed, then 0.1 part by weight of concentrated sulfuric acid is added while agitating at ambient temperature and pressure. The mixture is agitated for about 1 hour and the reaction is complete in 1 to 12 hours, thereby producing a light yellow, soft, solid, poly (methallyl chloride styrene) copolymer.
Workup
- stirringThe mixture is agitated for about 1 hour
Sources & evidence
- ORD record
- ord-aa8387462eef4c85b97655c81d0aceb4
- Source dataset
- uspto-grants-1980_05
- Patent number
- US04201702
Reaction notes
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