HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → Quinoline-4-carboxylic acid (alpha-methyl-delta-diethylaminobutyl)amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Novoldiamine | HCID 78953 | — |
| Reactant | Quinoline-4-carbonyl chloride hydrochloride | HCID 12373997 | — |
| Solvent | Water | HCID 962 | — |
| Product | Quinoline-4-carboxylic acid (alpha-methyl-delta-diethylaminobutyl)amide | HCID 86736974 | — |
Reaction Steps
2-[2'-(5"-nitrofuryl-2")vinyl]quinoline-4-carboxylic acid (α-methyl-δ-diethylaminobutyl)amide was prepared from 1.58 g (0.01 mol.) of diethylamino-4-aminopentane and 3.65 g (0.01 mol.) of 2-[2'-(5"-nitrofuryl-2")vinyl]quinoline-4-carboxylic acid chloride hydrochloride in 50 ml of water in the presence of triethylamine. The process was conducted as described in Example 5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04201784 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-b775b91c71bb4b2597ae21fb2ec7a4ff |
| Source note | uspto-grants-1980_05 |