Ammonia → HCID 86736684, compound

HRID 1395067Notes

Reaction equation

HRID 1395067 reaction equation
[Ag:1].[Cl:2][C:3]1[N:11]=[C:10]2[C:6]([NH:7][CH:8]=[N:9]2)=[C:5]([Cl:12])[N:4]=1.N>O>[Ag:1].[Cl:2][C:3]1[N:11]=[C:10]2[C:6]([NH:7][CH:8]=[N:9]2)=[C:5]([Cl:12])[N:4]=1

Participants

5

Reactant 3

HCID 222AmmoniaHCID 23954Silver2×HCID 53244122,6-Dichloropurine2×

Product 1

HCID 86736684HCID 86736684, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The silver derivative of 2,6-dichloropurine may be prepared according to the general procedure disclosed in J. Am. Chem. Soc., 73, 1650 (1951), i.e. the 2,6-dichloropurine is dissolved in boiling water, the solution is basified (e.g. with aqueous ammonia) and an aqueous solution of about one equivalent of a silver salt (e.g. AgNO3) is added to form the desired 2,6-dichloropurine silver salt.

Sources & evidence

ORD record
ord-7724cc4b530046adbc06196f52fcf7d9
Source dataset
uspto-grants-1980_05
Patent number
US04201860

Reaction notes

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