HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dinitrobenzene → HCID 20340131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dinitrobenzene | HCID 7452 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Catalyst | Cupric acetate | HCID 8895 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20340131 | HCID 20340131 | — |
Reaction Steps
A small amount of m-dinitrobenzene and copper(II) acetate were added whereupon a solution of 124.5 g of methacrylyl chloride (1 mole) in 125 ml of dioxan were added dropwise. The temperature was kept at 20°-25° C. Stirring was then continued for 30 min whilst slowly heating until reflux. Light yellow needles were sucked off, washed with ether, and dried under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04202697 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-f0a772888a5047acb8c6ec095c4b4066 |
| Source note | uspto-grants-1980_05 |