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HRID1395107

反应详情

EQUATION

反应方程式

HRID 1395107 的结构方程式

REACTANTS

反应物

3
结构：CC(C)Br
HCID6358

2-Bromopropane

C3H7Br

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：O=[N+]([O-])c1ccccc1S
HCID21002

o-Nitrobenzenethiol

C6H5NO2S

PRODUCTS

生成物

1
结构：CC(C)Sc1ccccc1[N+](=O)[O-]
HCID12505026

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

2-Nitrothiophenol, 2-bromopropane, potassium carbonate and acetone were refluxed for several hours. The solvent then was removed by rotary evaporation. The crude product was partitioned between methylene chloride and a 10% sodium carbonate solution. The organic phase was distilled to yield 2-isopropylmercaptonitrobenzene.

WORKUP

后处理

  1. customThe solvent then was removed by rotary evaporation
  2. customThe crude product was partitioned between methylene chloride
  3. distillationThe organic phase was distilled