2-Nitrophenol → HCID 54051739, compound

HRID 1395116Notes

Reaction equation

[CH2:1](Br)[CH:2]=[CH2:3].[N+:5]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[OH:14])([O-:7])=[O:6]>>[CH:3]([O:14][C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=1[N+:5]([O-:7])=[O:6])=[CH:2][CH3:1]

Participants

Reactant 2

HCID 69472-Nitrophenol

HCID 7841Allyl bromide

Product 1

HCID 54051739HCID 54051739, compound

Procedure

Allyl bromide was reacted with o-nitrophenol to yield 2-prop-1-en-oxynitrobenzene; which was reduced to the corresponding aniline; then reacted with 5-methyl-N-chloromethyl-2-pyrrolidone to form the corresponding 5-methyl-N'-methylene-2-pyrrolidonyl derivative.

Sources & evidence

ORD record: ord-ac46a4ddf84648548ff10ec7b8abefdf
Source dataset: uspto-grants-1980_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04202821

Reaction notes

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