2-Nitrophenol → HCID 57005160, compound
Reaction equation
[CH:1]1([OH:6])[CH2:5][CH:4]=[CH:3][CH2:2]1.[N+:7]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1O)([O-:9])=[O:8]>>[CH:1]1([O:6][C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[N+:7]([O-:9])=[O:8])[CH2:5][CH:4]=[CH:3][CH2:2]1Participants
3
Procedure
Cyclopent-3-en-1-ol was reacted with o-nitrophenol to yield 2-cyclopent-3-en-oxynitrobenzene; which was reduced to the corresponding aniline; then reacted with 5-methyl-N-chloromethyl-2-pyrrolidone to form the corresponding 5-methyl-N'-methylene-2-pyrrolidonyl derivative.
Sources & evidence
- ORD record
- ord-196431e2d205446e90770ad12ed4151d
- Source dataset
- uspto-grants-1980_05
- Patent number
- US04202821
Reaction notes
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