HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-3-[4-(2-methylbutan-2-yl)phenyl]prop-2-en-1-ol → 2-Methyl-3-[4-(2-methylbutan-2-yl)phenyl]propan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-3-[4-(2-methylbutan-2-yl)phenyl]prop-2-en-1-ol | HCID 57245577 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 2-Methyl-3-[4-(2-methylbutan-2-yl)phenyl]propan-1-ol | HCID 20340528 | — |
Reaction Steps
70 g of 3-(p-tert.amyl-phenyl)-2-methyl-allyl alcohol are dissolved in 700 ml of alcohol, treated with 7 g of 5% palladium/carbon and hydrogenated until the hydrogen uptake has been completed. The catalyst is subsequently filtered and the alcohol is evaporated. By distillation there is obtained pure 3-(p-tert.amyl-phenyl)-2-methyl-propanol of boiling point 124°-129° C./0.04 Torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04202894 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-a4457355c5234f16b2b7ac5c68dd416d |
| Source note | uspto-grants-1980_05 |