HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Methacrylate → Butyl Acrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | Butyl Acrylate | HCID 8846 | 97.6% |
Reaction Steps
The reaction was performed for two hours by adding 172.2 g (2.0 moles) of methyl acrylate in the apparatus of Example 1 instead of the methyl methacrylate. The results of the experiment were 98.4% conversion of n-butanol and 97.6% yield of n-butyl acrylate. When this ester was distilled in the same manner as in Example 1, it was recovered in a 96.6% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04202990 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-ade8ec79ce724b788c8c782eacc2c9f3 |
| Source note | uspto-grants-1980_05 |