Azane;hydrate → HCID 20339008, compound

Participants

Reaction Conditions

Reaction Steps

A 10 g of methyl-α-[2-cyano-5-(2-chloro-4-trifluoromethyl phenoxy)phenoxy]propionate was dissolved in 20 ml of benzene. The solution was cooled at 0° C. and 10 g of 28% ammonia water was added dropwise to react them at room temperature for 2 hours. After the reaction, the benzene phase was separated and was washed with water. The benzene was distilled off and the product was recrystallized from methanol to obtain 5.5 g of the object compound having a melting point of 134° to 137° C.

Provenance & Evidence