2-Nitrophenol → HCID 57005160, compound
Reaction equation
[CH:1]1([OH:6])[CH2:5][CH:4]=[CH:3][CH2:2]1.[N+:7]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1O)([O-:9])=[O:8]>>[CH:1]1([O:6][C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[N+:7]([O-:9])=[O:8])[CH2:5][CH:4]=[CH:3][CH2:2]1Participants
3
Procedure
Cyclo-pent-3-en-1-ol was reacted with o-nitrophenol to yield 2-cyclopent-3-en-oxy nitrobenzene; which was reduced to the corresponding aniline; then reacted with N-hydromethyl-5-methyl-2-pyrrolidone to form the corresponding N-5-methyl-N-methylene-2-pyrrolidonyl derivative.
Sources & evidence
- ORD record
- ord-b2bea809fe04407c8c25876656a1edd9
- Source dataset
- uspto-grants-1980_05
- Patent number
- US04203901
Reaction notes
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