HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargylamine → HCID 136023135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargylamine | HCID 239041 | — |
| Reactant | N-cyano-N'-{2-[(5-methylaminomethyl-2-furyl)methylthio]ethyl}-S-methylisothiourea | HCID 20339222 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 136023135 | HCID 136023135 | — |
Reaction Steps
A mixture of N-cyano-N'-{2-[(5-methylaminomethyl-2-furyl)methylthio]ethyl}-S-methylisothiourea [prepared according to the procedure described in Belgian Pat. No. 857,388] and propargylamine in methanol is stirred and heated under a positive pressure of nitrogen to give, after workup and chromatography, the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04203909 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-7383cece77b44642ad08617167eadc7a |
| Source note | uspto-grants-1980_05 |