HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylphosphite → 1-Carbomethoxymethyl-2-Diethoxyphosphoryl Hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylphosphite | HCID 3780918 | — |
| Reactant | 1-Acetyl-1-Methyl-2-Diethoxyphosphoryl Hydrazine | HCID 20339292 | — |
| Reactant | 2-(2-Methylhydrazinyl)acetic acid;hydrochloride | HCID 71437528 | — |
| Product | 1-Carbomethoxymethyl-2-Diethoxyphosphoryl Hydrazine | HCID 20339293 | — |
Reaction Steps
This compound was synthesized in a similar manner to the compound of Example 5, except that methylhydrazinoacetate hydrochloride was used in place of 1-acetyl-1-methyl hydrazine and diethylphosphite was used in place of dimethylphosphite. A colorless oil was obtained which was subsequently distilled at 115° C./0.05 mm. to yield the desired product, nD27 =1.4342.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04203932 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-ce30004598534f7686ed1267d82c77a3 |
| Source note | uspto-grants-1980_05 |