HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Bromide → HCID 20337882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Bromide | HCID 6323 | — |
| Reactant | HCID 12519327 | HCID 12519327 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20337882 | HCID 20337882 | — |
Reaction Steps
In 5 ml. of acetone was dissolved 0.5 g. of 2-(dithien-2-ylmethylene)quinolizidine. To the resulting solution was added 2.0 ml. of methyl bromide. The mixture was stirred at room temperature for 24 hrs. The formed crystals were taken out by filtration. By recrystallizing from ethanol, 0.49 g. of colorless crystals showing a melting point of 246°-248° C. (decomposed) were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04205074 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-2878aec8cb86409d8782ee09a0c956a4 |
| Source note | uspto-grants-1980_05 |