反应详情

A mixture of 5-hydroxyanthranilamide (15.2 g), 250 ml water, 5.1 ml 50% NaOH, and 11.7 ml benzyl chloride was heated 1/2 hour at 95°, filtered and the solid recrystallized from 200 ml butanol to give 16.6 g product, m.163-5.

1. temperaturewas heated 1/2 hour at 95°
2. filtrationfiltered
3. customthe solid recrystallized from 200 ml butanol