HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilamide → HCID 11345158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilamide | HCID 6942 | — |
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 11345158 | HCID 11345158 | — |
Reaction Steps
To a hot solution of 20 g NaOH in 1250 ml water was added 68 g 2-aminobenzamide followed by 58 ml benzyl chloride. The mixture was refluxed 20 minutes, cooled and the solid filtered and washed with water. The product was recrystallized from 95% alcohol to give 62 g, m.169-73.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04205173 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-598f4ebf0c6a49d896c5d0620355793b |
| Source note | uspto-grants-1980_05 |