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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1395962생성일: 2026년 10월 27일

Ethanol → Sodium 1,3,5-tricyclohexylbenzenesulfonate

https://huagongshe.com/reaction/1395962

반응식

참여 물질

역할이름HCID투입량
반응물EthanolHCID 702—
반응물Sodium HydroxideHCID 14798—
반응물Chlorosulfonic acidHCID 24638—
반응물TricyclohexylbenzeneHCID 3015433—
용매DichloromethaneHCID 6344—
생성물Sodium 1,3,5-tricyclohexylbenzenesulfonateHCID 86655172—

반응 조건

온도3 °C

반응 단계

Tricyclohexylbenzene amounting to 30 g was dissolved in 50 ml of methylene chloride, and agitated while cooling at 3° C. Then, 15.2 g of chlorosulfonic acid was slowly dropped thereinto. After the completion of the dropping, the mixture was agitated at room temperature for 5 hours, and 10 g of ice was poured thereinto. Further, 40 g of a 50% aqueous solution of sodium hydroxide was poured into the mixture, and 20 g of ethanol was added thereto. The mixture was agitated at 50° C. for 1 hour, and any undissolved matter was removed by filtration. Vacuum distillation was carried out at 40° C., and separated crystals were collected by filtration. The crystals were washed with hexane. Thus, 30 g of sodium 1,3,5-tricyclohexylbenzenesulfonate was obtained.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08900791B2
출처 데이터셋uspto-grants-2014_12
ORD IDord-a8e0a94e45e64799a2c217734f46777e
출처 메모uspto-grants-2014_12