HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sarcosine → HCID 66632673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sarcosine | HCID 1088 | — |
| Reactant | 3-Methyl-2-butenal | HCID 61020 | — |
| Reactant | HCID 759029 | HCID 759029 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 66632673 | HCID 66632673 | — |
Reaction Steps
A mixture of 3-E-3-benzylidene-1,3-dihydro-indol-2-one (10.0 mmol), N-methyl-glycine (14 mmol) and 3-methyl-but-2-enal (14 mmol) in 100 mL toluene was refluxed for 6 hours. The solvent was removed and the residue was purified on silica gel column to yield the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901117B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-67e8717a49c649e2b014f3140bfbefaa |
| Source note | uspto-grants-2014_12 |