HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyaniline → HCID 178490983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Reactant | HCID 178418413 | HCID 178418413 | — |
| Solvent | 1-Pentanol | HCID 6276 | — |
| Product | HCID 178490983 | HCID 178490983 | — |
Reaction Steps
4-Hydroxy-2-(methylthio)pyrimidine-5-carbonitrile (3 mmol) and m-anisidine (3 mmol) in pentan-1-ol was refluxed for 40 h under nitrogen. The reaction mixture was concentrated in vacuo. The residue was washed with water and dried to afford 4-hydroxy-2-(3-methoxyphenylamino)pyrimidine-5-carbonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901143B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-40218cd3e9d248a39583346e7891bdb4 |
| Source note | uspto-grants-2014_12 |