Methanol → HCID 178507920, compound

Participants

Reaction Steps

A rb flask equipped with a stirring bar was charged with 4-aminopyrimidine (462 mg, 4.86 mmol) in dichloromethane (DCM) (25 mL). To this was added m-CPBA (1198 mg, 5.34 mmol). After 2, the mixture was concentrated and purified by washing through a pad of silica eluting with 80:20:1:DCM:MeOH:NH4OH to afford 350 mg (3.15 mmol, 65%) of the title compound. LC/MS: (M+H)+: 111.8.

Provenance & Evidence