N,N-Dimethylaminoethyl chloride hydrochloride → HCID 67323446, compound

Participants

Reaction Steps

This compound was synthesized from 2-(2-(4-fluorophenyl)oxazol-4-yl)acetonitrile and 2-chloro-N,N-dimethylethanamine hydrochloride as described in example 16 step 1b (400 mg, yield 48%). 1H NMR (400 MHz, MeOD) δ 8.10-8.07 (m, 2H), 7.99 (m, 1H), 7.29-7.25 (t, J=8.9 Hz, 2H), 4.24-4.20 (t, J=7.3 Hz, 1H), 2.59-2.46 (m, 2H), 2.29 (s, 6H), 2.23-2.17 (m, 2H). MS (ESI) m/z: Calculated for C15H16FN3O: 273.13. found: 274.2 (M+H)+.

Provenance & Evidence