HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(5-(Trifluoromethyl)-1,2,4-oxadiazol-3-yl)benzoic acid → HCID 53345017, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(5-(Trifluoromethyl)-1,2,4-oxadiazol-3-yl)benzoic acid | HCID 25180854 | — |
| Reactant | HCID 178448774 | HCID 178448774 | — |
| Product | HCID 53345017 | HCID 53345017 | 11% |
Reaction Steps
This compound was synthesized from 2-methyl-2-(5-phenyl-1H-pyrazol-3-yl)propan-1-amine and 3-(5-(trifluoromethyl)-1,2,4-oxadiazol-3-yl)benzoic acid as described in example 8 step 6 (10 mg, yield 11%). 1H NMR (CDCl3) δ 8.52 (s, 1H) 8.20 (d, J=7.4, 1H), 8.05 (d, J=7.4, 1H), 7.64-7.52 (m, 3H), 7.46-7.32 (m, 3H), 6.47 (s, 1H), 3.70 (d, J=4.5, 2H), 1.44 (s, 6H). MS (ESI) m/z: Calculated for C23H20F3N5O2: 455.16. found: 456.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901156B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-95cb6e5954214faf88485fc3cbf0f9ff |
| Source note | uspto-grants-2014_12 |