HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Carboxyphenylboronic acid → HCID 67323228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Carboxyphenylboronic acid | HCID 2733957 | — |
| Reactant | 1-(5-Bromothiophen-3-yl)-2,2,2-trifluoroethan-1-one | HCID 67324122 | — |
| Product | HCID 67323228 | HCID 67323228 | 16% |
Reaction Steps
This compound was synthesized from 1-(5-bromothiophen-3-yl)-2,2,2-trifluoroethanone and 3-carboxyphenylboronic acid as described in example 88 step 3 (150 mg, yield 16%) as a yellow solid. 1H NMR (300 MHz, DMSO-d6) δ 13.26 (br s, 1H), 8.85 (s, 1H), 8.19 (s, 1H), 8.07-8.05 (m, 2H), 7.96-7.93 (d, J=7.9 Hz, 1H), 7.62-7.57 (t, J=7.7 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901156B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-c9ad1765823047ca8c59e2d5bd074706 |
| Source note | uspto-grants-2014_12 |