Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 5-Amino-4,6-dichloropyrimidine | HCID 79434 | — |
| Product | HCID 12611968 | HCID 12611968 | — |
Reaction Steps
A mixture of 5-amino-4,6-dichloropyrimidine (1.15 g, 0.00701 mol) and benzoyl chloride (1.0 mL, 0.0086 mol) was heated at 100° C. overnight. The reaction was cooled and the residue was triturated with diethyl ether, filtered and collected to obtain 1.6 g (85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08901136B2 |
|---|
| Source dataset | uspto-grants-2014_12 |
|---|
| ORD ID | ord-1e6b5706f435499b858f0ee2c9429ed0 |
|---|
| Source note | uspto-grants-2014_12 |
|---|
