HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → (8-Methyl-2-o-tolylquinolin-3-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 57707895 | HCID 57707895 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | (8-Methyl-2-o-tolylquinolin-3-yl)methanol | HCID 57707986 | — |
Reaction Steps
Prepared according to Procedure B using 8-methyl-2-o-tolylquinoline-3-carb-aldehyde (1.28 g, 4.9 mmol) and solid NaBH4 (278 mg, 1.5 eq) in THF (10 mL). After purification, (8-methyl-2-o-tolylquinolin-3-yl)methanol was obtained as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901135B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-3c84b80f0ab1418aae1896c639319c18 |
| Source note | uspto-grants-2014_12 |