2-Methoxyphenylhydrazine Hydrochloride → HCID 73291874, compound

HRID 1398043Notes

Reaction equation

HRID 1398043 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5](/[C:8](/O)=[CH:9]/[C:10]([CH:12]2[CH2:17][CH2:16][O:15][C:14]([CH3:19])([CH3:18])[CH2:13]2)=O)=[CH:4][CH:3]=1.Cl.[CH3:22][O:23][C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=1[NH:30][NH2:31]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:30]([C:25]3[CH:26]=[CH:27][CH:28]=[CH:29][C:24]=3[O:23][CH3:22])[N:31]=[C:10]([CH:12]3[CH2:17][CH2:16][O:15][C:14]([CH3:19])([CH3:18])[CH2:13]3)[CH:9]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 28494452-Methoxyphenylhydrazine HydrochlorideHCID 86722006HCID 86722006, compound

Product 1

HCID 73291874HCID 73291874, compound

Procedure

The title compound was prepared from (Z)-3-(4-chlorophenyl)-1-(2,2-dimethyltetrahydro-2H-pyran-4-yl)-3-hydroxyprop-2-en-1-one and (2-methoxyphenyl)hydrazine hydrochloride according to the procedure in Example 50, step B.

Sources & evidence

ORD record
ord-c201bf2011304487a893f3b2be8a0eaa
Source dataset
uspto-grants-2014_12
Patent number
US08901314B2

Reaction notes

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