反应详情

The title compound was prepared by the procedure described in Step 2 of Example 142-b by reacting 4-(6-bromo-2-ethoxy-1,3-benzodiazol-1-yl)pyrimidin-2-amine with 2-methyl-3-butyn-2-ol; 1H NMR (500 MHz, MeOD) delta 1.54 (3H, t, J=7.09 Hz), 1.58 (6H, s), 4.68 (2H, q, J=7.09 Hz), 7.11 (1H, d, J=5.67 Hz), 7.25-7.32 (1H, m), 7.39 (1H, d, J=8.20 Hz), 8.29 (1H, s), 8.31-8.43 (1H, m); LC-MS: m/z=+338.5 (M+H)+.