Methyl iodide → HCID 178481990、化合物

関与物質

反応条件

反応手順

1-benzyl-4-phenyl-1H-1,2,3-triazole (0.52 g, 2.20 mmol) prepared above and iodomethane (2 ml, 32.0 mmol) were added to a 20 mL vial. The reaction was heated at 40° C. for 3 days. The iodomethane was allowed to evaporate in the hood. The crude product was dissolved with 2 mL CH2Cl2 under reflux. The solution was precipitated into a mixture of acetone, ethyl acetate and hexane. The yellow solid was collected and dried in vacuo.

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