Methyl iodide → HCID 178444686, compound

HRID 1399384Notes

Reaction equation

HRID 1399384 reaction equation
[CH2:1]([N:7]1[CH:11]=[C:10]([CH2:12][CH2:13][CH3:14])[N:9]=[N:8]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[I:15][CH3:16]>>[I-:15].[CH2:1]([N:7]1[CH:11]=[C:10]([CH2:12][CH2:13][CH3:14])[N+:9]([CH3:16])=[N:8]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Participants

3

Reactant 2

HCID 6328Methyl iodide2×HCID 89528143HCID 89528143, compound

Product 1

HCID 178444686HCID 178444686, compound

Conditions

Temperature
40 °C

Procedure

1-hexyl-4-propyl-1H-1,2,3-triazole and excess iodomethane were added to a 20 mL vial. The reaction was heated at 40° C. for 3 days. The iodomethane was allowed to evaporate in the hood. The following structure of 1-hexyl-3-methyl-4-propyl-1H-1,2,3-triazol-3-ium iodide was confirmed:

Workup

  1. customto evaporate in the hood

Sources & evidence

ORD record
ord-77348339f0f34eeb87738e2c3e9a2d42
Source dataset
uspto-grants-2014_12
Patent number
US08906135B1

Reaction notes

Loading…