5-Methylfurfural → 2-[(1-chloronaphthalen-2-yl)oxy]-N-[(5-methylfuran-2-yl)methyl]ethanaminium chloride

HRID 1400248Notes

Reaction equation

HRID 1400248 reaction equation
[Cl-].[Cl:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][C:4]=1[O:13][CH2:14][CH2:15][NH3+:16].[CH3:17][C:18]1[O:22][C:21]([CH:23]=O)=[CH:20][CH:19]=1>>[Cl-:2].[Cl:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][C:4]=1[O:13][CH2:14][CH2:15][NH2+:16][CH2:23][C:21]1[O:22][C:18]([CH3:17])=[CH:19][CH:20]=1

Participants

3

Reactant 2

HCID 120975-MethylfurfuralHCID 681514342-[(1-Chloronaphthalen-2-yl)oxy]ethanaminium chloride

Product 1

HCID 867097502-[(1-chloronaphthalen-2-yl)oxy]-N-[(5-methylfuran-2-yl)methyl]ethanaminium chlorideYield 70%

Procedure

Prepared from 2-[(1-chloronaphthalen-2-yl)oxy]ethanaminium chloride and 5-methylfuran-2-carbaldehyde in 70% yield as a white solid.

Sources & evidence

ORD record
ord-78dac9be12e9400eb295ac188267fde9
Source dataset
uspto-grants-2014_12
Patent number
US08906946B2

Reaction notes

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