2-Acetyl-5-Methylfuran → N-{2-[(1-chloronaphthalen-2-yl)oxy]ethyl}-1-(5-methylfuran-2-yl)ethanamine

HRID 1400249Notes

Reaction equation

HRID 1400249 reaction equation
[Cl-].[Cl:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][C:4]=1[O:13][CH2:14][CH2:15][NH3+:16].[CH3:17][C:18]1[O:22][C:21]([C:23](=O)[CH3:24])=[CH:20][CH:19]=1>>[Cl:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][C:4]=1[O:13][CH2:14][CH2:15][NH:16][CH:23]([C:21]1[O:22][C:18]([CH3:17])=[CH:19][CH:20]=1)[CH3:24]

Participants

3

Reactant 2

HCID 145142-Acetyl-5-MethylfuranHCID 681514342-[(1-Chloronaphthalen-2-yl)oxy]ethanaminium chloride

Product 1

HCID 59053531N-{2-[(1-chloronaphthalen-2-yl)oxy]ethyl}-1-(5-methylfuran-2-yl)ethanamineYield 34%

Procedure

Prepared from 2-[(1-chloronaphthalen-2-yl)oxy]ethanaminium chloride and 1-(5-methylfuran-2-yl)ethanone in 34% yield as a pale yellow oil.

Sources & evidence

ORD record
ord-39b0d837722f4ee4b8e623ee27ac257b
Source dataset
uspto-grants-2014_12
Patent number
US08906946B2

Reaction notes

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