2-Thiophenecarboxaldehyde, 5-chloro- → HCID 59054437, compound

HRID 1400266Notes

Reaction equation

HRID 1400266 reaction equation
[Cl:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[O:12][CH2:13][CH:14]([NH2:16])[CH3:15].[Cl:17][C:18]1[S:22][C:21]([CH:23]=O)=[CH:20][CH:19]=1>>[Cl:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[O:12][CH2:13][CH:14]([NH:16][CH2:23][C:21]1[S:22][C:18]([Cl:17])=[CH:19][CH:20]=1)[CH3:15]

Participants

3

Reactant 2

HCID 817002-Thiophenecarboxaldehyde, 5-chloro-HCID 68151515HCID 68151515, compound

Product 1

HCID 59054437HCID 59054437, compoundYield 61%

Procedure

Prepared from 1-[(1-chloronaphthalen-2-yl)oxy]propan-2-amine and 5-chlorothiophen-2-carbaldehyde in 61% yield as a slightly white oil.

Sources & evidence

ORD record
ord-09b3bad585344df6bb6234d773382a32
Source dataset
uspto-grants-2014_12
Patent number
US08906946B2

Reaction notes

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