HCID 59054439, compound → HCID 59054441, compound

HRID 1400270Notes

Reaction equation

HRID 1400270 reaction equation
[Cl:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[S:12]([CH2:15][CH2:16][NH:17][CH2:18][C:19]1[O:20][CH:21]=[CH:22][CH:23]=1)(=[O:14])=[O:13].[Cl:24]C1OC(CNCCSC2C=CC3C(=CC=CC=3)C=2Cl)=CC=1>>[Cl:24][C:21]1[O:20][C:19]([CH2:18][NH:17][CH2:16][CH2:15][S:12]([C:3]2[CH:4]=[CH:5][C:6]3[C:11](=[CH:10][CH:9]=[CH:8][CH:7]=3)[C:2]=2[Cl:1])(=[O:14])=[O:13])=[CH:23][CH:22]=1

Participants

3

Reactant 2

HCID 59054439HCID 59054439, compoundHCID 68151646HCID 68151646, compound

Product 1

HCID 59054441HCID 59054441, compoundYield 50%

Procedure

Prepared as described for compound 25 from N-[(5-chlorofuran-2-yl)methyl]-2-[(1 chloronaphthalen-2-yl)sulfanyl]ethanamine in 50% yield as whitish solid.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-8159d3e142e043848b8e453bfc4b4450
Source dataset
uspto-grants-2014_12
Patent number
US08906946B2

Reaction notes

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